ASTM D2892 D5236 Semi-Automatic Fractional Crude Oil Distillation Specifications

 

Semi Automatic D2892 D5236 Crude Oil Distillation

Automatic Control:

 

  • Fraction Collector
  • Vacuum Control
  • Condenser Temperature
  • Reflux Ratio
  • AET Temperature Calculation
  • Distillation Column Heated Jacket Control
  • Recording of Distillation Data
  • Distillation Rate Control
  • Ending of Distillation and Cool Down

Semi-Automatic Control:

  • Heat Control for Boiling Flask

Operator Controlled:

  • Measurement of Receiver Volume
  • Creating Volume vs Temperature Distillation Curve

Boiling Flask/Heating Mantle:

  • Stirring Heating Mantle
  • Heated Mantle Top
  • Stainless Steel Boiling Flask (optional glass flasks available)
  • Quench Coil for Rapid Cooling of the Flask Contents
  • PRT Temperature Probe to Monitor Boiling Flask Temperature
  • Boiling Flask Sizes 1, 2, 3, 6, 12, 22, 30, 50, 100 liters (Other sizes available)

ASTM D2892 Distillation Column:

  • According ASTM specifications
  • Vertical viewing window for easy viewing
  • Highly reflective vacuum jacket
  • Heated Jacket to Prevent Heat Loss (Automatically Controlled)
  • 15 Theoretical Plates (Other Efficiencies Available)

ASTM D2892 Distillation Column Sizes, Propak:

Diameter Packed Height Sample Range
70 mm 91 cm 15-60 liters
50 mm 80 cm 6-24 liters
25 mm 57 cm 1.2-4.8 liters

Other D2892 Distillation Columns:

  • We also offer distillation columns packed with mesh packing (Goodloe) and real plate distillation columns.

ASTM D5236 Distillation Column Sizes:

Diameter Boiling Flask Sample Range
70 mm 12-24 liters 8-16 liters
50 mm 6-12 liters 4-8 liters
36 mm 3-6 liters 2-4 liters
25 mm 2-3 liters 1-2 liters

Fraction Collector

  • 8 Fractions at Each Pressure Level
  • Automatic Collection by Vapor Temperature
  • Graduate Receivers (10, 25, 50, 100 ,250, 500, 1000, 2000, 5000 ml)

Circulating Bath

  • Automatic control from PC
  • Programmable
  • -20 – 100 °C
  • Low liquid cut off
  • Over temperature cut off

Vacuum Operation

  • Automatic control
  • Programmable

Vacuum Components

  • 100-1 mmHg range standard (MKS)
  • 1-0.1 mmHg range (MKS)
  • Optional 760-100 mmHg range (MKS)
  • Automatic control valve (MKS)
  • Vacuum pump (Edwards)

Cold Trap

  • Cooling by dry ice
  • Optional automatic cooler

PC/Monitor

  • Included with distillation unit

Dimensions

  • 245 cm x 92 cm x 156 cm (H x D x W)

Power (Distillation Unit Only)

  • 220 VAC, 50/60 Hz

 

See our crude oil dehydration system